(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

Base Information

Chemical Name:(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol
CAS No.:1039740-24-3
Molecular Formula:C₁₃H₂₄O₄
Molecular Weight:244.331
Hs Code.:

Synonyms:(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

Suppliers and Price of (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

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Technology Process of (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

There total 1 articles about (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1039740-22-1
(1R,5S,8S)-8-(2,2-dimethoxyethyl)-8-methyl-2-methylen-6-oxabicyclo[3.2.1]octan-7-one

: 1039740-24-3
(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃;
DOI:10.1021/jo800913x

Reference yield: 85.0%

: 1039740-24-3
(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

: 824-94-2
p-methoxybenzyl chloride

: 1039740-26-5
(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at -60 - 20 ℃; for 12h;
DOI:10.1021/jo800913x