4'-methylacetophenone carbo-t-butoxyhydrazone

Base Information

Chemical Name:4'-methylacetophenone carbo-t-butoxyhydrazone
CAS No.:60295-09-2
Molecular Formula:C₁₄H₂₀N₂O₂
Molecular Weight:248.325
Hs Code.:

Synonyms:4'-methylacetophenone carbo-t-butoxyhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-methylacetophenone carbo-t-butoxyhydrazone

Chemical Property:

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Technology Process of 4'-methylacetophenone carbo-t-butoxyhydrazone

There total 2 articles about 4'-methylacetophenone carbo-t-butoxyhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 122-00-9
para-methylacetophenone

: 60295-09-2
4'-methylacetophenone carbo-t-butoxyhydrazone

Guidance literature:: para-methylacetophenone; With acetic acid; In ethanol; for 0.25h; Reflux;

t-butoxycarbonylhydrazine; In ethanol; Reflux;
DOI:10.1002/adsc.201600900

Reference yield:

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 122-00-9
para-methylacetophenone

: 60295-09-2
4'-methylacetophenone carbo-t-butoxyhydrazone

Guidance literature:: In ethanol;
DOI:10.1021/jo00886a007

Reference yield: 98.0%

: 6773-29-1
dimethyl diazomalonate

: 60295-09-2
4'-methylacetophenone carbo-t-butoxyhydrazone

: methyl 2-amino-1,6-dimethyl-3-oxo-2,3-dihydroisoquinolin-4-carboxylate

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; acetic acid; In 2,2,2-trifluoroethanol; at 80 ℃; for 12h; Reagent/catalyst; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.7b02066