dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

Base Information

Chemical Name:dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate
CAS No.:1040377-42-1
Molecular Formula:C₂₁H₂₂O₄
Molecular Weight:338.403
Hs Code.:

Synonyms:dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

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Chemical Property of dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

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Technology Process of dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

There total 3 articles about dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1187250-79-8
C₁₆H₁₆O₂

: 762-42-5
dimethyl acetylenedicarboxylate

: 1040377-42-1
dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

Guidance literature:: In para-xylene; at 180 ℃; for 24h; Sealed tube;
DOI:10.1016/j.tetlet.2009.06.124

Reference yield: 84.0%

: 1040377-25-0
ethyl 2-acetyl-8-phenyloct-7-ynoate

: 762-42-5
dimethyl acetylenedicarboxylate

: 1040377-42-1
dimethyl 3-methyl-4-phenyl-5,6,7,8-tetrahydronaphthalene-1,2-dicarboxylate

Guidance literature:: ethyl 2-acetyl-8-phenyloct-7-ynoate; With bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer; In toluene; at 150 ℃; for 24h; Molecular sieve; Inert atmosphere;

dimethyl acetylenedicarboxylate; In toluene; at 150 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo902072q