5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene

Base Information

• Chemical Name: 5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene
• CAS No.: 850537-86-9
• Molecular Formula: C₈₄H₈₀O₁₆
• Molecular Weight: 1345.55

Synonyms:5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene

Chemical Property of 5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene

Chemical Property:

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Technology Process of 5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene

There total 1 articles about 5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

4-Formylphenyl acrylate (41704-79-4) + 5,11,17,23-tetraiodocalix[4]arene-25,26,27,28-tetra-n-butyl ether (420115-28-2,340819-87-6) → 5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene (850537-86-9)

Guidance literature:

With triethylamine; diphenylphosphinopropane; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 48h;

DOI:10.1016/j.tetlet.2005.01.168

Reference yield: 88.0%

5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene (850537-86-9) + benzylamine (100-46-9) → C112H108N4O12

Guidance literature:

With molecular sieve; In chloroform;

DOI:10.1016/j.tetlet.2005.01.168

Reference yield: 80.0%

5,11,17,23-tetrakis[(E)-2-(4-formylphenoxycarbonyl)ethenyl]-25,26,27,28-tetrabutoxycalix[4]arene (850537-86-9) + 4-methoxy-aniline (104-94-9) → C112H108N4O16

Guidance literature:

With molecular sieve; In chloroform;

DOI:10.1016/j.tetlet.2005.01.168

upstream raw materials:

4-Formylphenyl acrylate

5,11,17,23-tetraiodocalix[4]arene-25,26,27,28-tetra-n-butyl ether

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