4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

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Chemical Name:4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide
CAS No.:1415312-47-8
Molecular Formula:C₁₃H₁₆N₄O₃S
Molecular Weight:308.361
Hs Code.:

Synonyms:4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

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Chemical Property of 4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

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Technology Process of 4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

There total 2 articles about 4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1415312-45-6
2-(tetrahydro-2H-pyran-2-yl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-1,2,3-triazole

: 701-34-8
4-bromo-benzenesulfonic acid amide

: 1415312-47-8
4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; cesium fluoride; In methanol; at 120 ℃; for 0.333333h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tetlet.2012.10.034

Reference yield:

: 1415312-44-5
2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazole

: 1415312-47-8
4-(2-(tetrahydro-2H-pyran-2-yl)-2H-1,2,3-triazol-4-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / pentane / 0.25 h / Inert atmosphere

1.2: 16 h / 25 °C / Inert atmosphere

2.1: cesium fluoride; bis-triphenylphosphine-palladium(II) chloride / methanol / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; cesium fluoride; 4,4'-di-tert-butyl-2,2'-bipyridine; In methanol; pentane; 2.1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tetlet.2012.10.034