(E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

Base Information

Chemical Name:(E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate
CAS No.:1206796-09-9
Molecular Formula:C₂₁H₁₇N₇O₃
Molecular Weight:415.411
Hs Code.:

Synonyms:(E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

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Chemical Property of (E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

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Technology Process of (E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

There total 1 articles about (E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1517-05-1
2-azidoethanol

: 32315-10-9
bis(trichloromethyl) carbonate

: (E)-2-(4-(4'-aminophenylethenyl)-3-cyano-5,5-dimethyl-5H-furan-2-ylidene)-malononitrile

: 1206796-09-9
(E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

Guidance literature:: bis(trichloromethyl) carbonate; (E)-2-(4-(4'-aminophenylethenyl)-3-cyano-5,5-dimethyl-5H-furan-2-ylidene)-malononitrile; With pyridine; In tetrahydrofuran; dichloromethane; for 2h; Cooling with ice; Inert atmosphere;

2-azidoethanol; With triethylamine; In tetrahydrofuran; dichloromethane; for 2h;
DOI:10.1039/b917119n

Reference yield: 90.0%

: 1206796-08-8
(E)-2-(4-(4-(but-3-ynylamino)styryl)-3-cyano-5,5-dimethylfuran-2(5H)-ylidene)malononitrile

: 1206796-09-9
(E)-2-azidoethyl 4-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

: 1206796-07-7
2-(4-(2-(4-((E)-2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylamino)ethyl)-1H-1,2,3-triazol-1-yl)ethyl 4-((E)-2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)phenylcarbamate

Guidance literature:: With (BimC₄A)3; copper(II) sulfate; sodium L-ascorbate; In methanol; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b917119n