4-octyl-p-acetylphenyltriazene

Base Information Edit

Chemical Name:4-octyl-p-acetylphenyltriazene
CAS No.:82834-22-8
Molecular Formula:C₁₆H₂₅N₃O
Molecular Weight:275.394
Hs Code.:
Mol file:82834-22-8.mol

Synonyms:4-octyl-p-acetylphenyltriazene

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Chemical Property of 4-octyl-p-acetylphenyltriazene Edit

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Technology Process of 4-octyl-p-acetylphenyltriazene

There total 5 articles about 4-octyl-p-acetylphenyltriazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-63-9
octan-4-one

: 82834-22-8
4-octyl-p-acetylphenyltriazene

Guidance literature:: Multi-step reaction with 3 steps

1: 90.5 percent / hydroxylamine hydrochloride, sodium hydroxide / H₂O / 6 h / Heating

2: sodium

3: sodium carbonate / acetonitrile / 1) (-10) deg C - (-5) deg C, 10 min; 2) 20 min

With sodium hydroxide; hydroxylamine hydrochloride; sodium; sodium carbonate; In water; acetonitrile;

Reference yield:

: 7207-51-4
octan-4-one oxime

: 82834-22-8
4-octyl-p-acetylphenyltriazene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium

2: sodium carbonate / acetonitrile / 1) (-10) deg C - (-5) deg C, 10 min; 2) 20 min

With sodium; sodium carbonate; In acetonitrile;

Reference yield:

: 589-62-8
octan-4-ol

: 82834-22-8
4-octyl-p-acetylphenyltriazene

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium dichromate, 98 percent sulphuric acid; 2) phthalic anhydride / 1) ether, water, 25-35 deg C, 2 h; 2) 100 deg C, 12 h

2: 90.5 percent / hydroxylamine hydrochloride, sodium hydroxide / H₂O / 6 h / Heating

3: sodium

4: sodium carbonate / acetonitrile / 1) (-10) deg C - (-5) deg C, 10 min; 2) 20 min

With sodium hydroxide; phthalic anhydride; sodium dichromate; sulfuric acid; hydroxylamine hydrochloride; sodium; sodium carbonate; In water; acetonitrile;