(Z)-but-2-enyl Cbz-glycinate

Base Information

Chemical Name:(Z)-but-2-enyl Cbz-glycinate
CAS No.:416898-31-2
Molecular Formula:C₁₄H₁₇NO₄
Molecular Weight:263.293
Hs Code.:

Synonyms:(Z)-but-2-enyl Cbz-glycinate

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Chemical Property of (Z)-but-2-enyl Cbz-glycinate

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Technology Process of (Z)-but-2-enyl Cbz-glycinate

There total 2 articles about (Z)-but-2-enyl Cbz-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 416898-31-2
(Z)-but-2-enyl Cbz-glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / DCC; DMAP / diethyl ether / 22 h / 20 °C

2: 89 percent / H₂; pyridine / Pd/CaCO₃ / ethyl acetate / 0.67 h / 20 °C

With pyridine; dmap; hydrogen; dicyclohexyl-carbodiimide; Lindlar's catalyst; In diethyl ether; ethyl acetate; 2: Lindlar reduction;
DOI:10.1039/b108752e

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 416898-31-2
(Z)-but-2-enyl Cbz-glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: EDCI; DMAP / CH₂Cl₂ / 0 °C

2: H₂ / Lindlar catalyst / methanol / 20 °C

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Lindlar's catalyst; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.03.078