3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide

Base Information

• Chemical Name: 3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide
• CAS No.: 1125465-82-8
• Molecular Formula: C₁₄H₁₃NO₅
• Molecular Weight: 275.261
• Mol file: 1125465-82-8.mol

Synonyms:3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide

Chemical Property of 3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide

Chemical Property:

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Technology Process of 3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide

There total 1 articles about 3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H19NO5 → 3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide (1125465-82-8)

Guidance literature:

With hydrogenchloride; water; acetic acid; for 120h;

DOI:10.1021/jm8013212

Reference yield: 76.0%

3-hydroxy-N-(2-methoxybenzyl)-4-oxo-4H-pyran-2-carboxamide (1125465-82-8) → 3-hydroxy-N-(2-methoxybenzyl)-4-thioxo-4H-pyran-2-carboxamide (1125465-83-9) + 3-hydroxy-N-(2-methoxybenzyl)-4-thioxo-4H-pyran-2-carbothioamide (1125465-84-0)

Guidance literature:

With tetraphosphorus decasulfide; Hexamethyldisiloxane; In benzene; at 105 ℃; for 2.5h;

DOI:10.1021/jm8013212

Downstream raw materials:

3-hydroxy-N-(2-methoxybenzyl)-4-thioxo-4H-pyran-2-carboxamide

3-hydroxy-N-(2-methoxybenzyl)-4-thioxo-4H-pyran-2-carbothioamide