Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

Base Information

Chemical Name:Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester
CAS No.:1296134-54-7
Molecular Formula:C₁₆H₂₀N₂O₁₀P₂
Molecular Weight:462.29
Hs Code.:

Synonyms:Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

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Chemical Property of Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

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Technology Process of Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

There total 3 articles about Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1296133-39-5
carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

: 118072-93-8
1-hydroxy-2-(imidazol-1-yl)ethylidene-1,1-bisphosphonic acid

: 1296134-54-7
Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

Guidance literature:: 1-hydroxy-2-(imidazol-1-yl)ethylidene-1,1-bisphosphonic acid; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 42 ℃; for 0.25h;

carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester; In N,N-dimethyl-formamide; at 40 - 42 ℃; for 24h;

In acetonitrile;

Reference yield:

: 90-02-8
salicylaldehyde

: 1296134-54-7
Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / toluene; acetonitrile / 1 h / 28 °C

2.1: pyridine; bis(trichloromethyl) carbonate / toluene / 1.5 h / 6.3 - 40 °C / Inert atmosphere

2.2: 10 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 42 °C

3.2: 24 h / 40 - 42 °C

3.3: Amberlite IR-120 (Na)

With pyridine; bis(trichloromethyl) carbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1296132-70-1
2-(isopropoxycarbonyloxy)benzaldehyde

: 1296134-54-7
Carbonic acid isopropyl ester 2-(2,3,4-trihydroxy-3-imidazol-1-ylmethyl-2,4-dioxo-2λ5,4λ5-[1,5,2,4]dioxadiphosphinan-6-yl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; bis(trichloromethyl) carbonate / toluene / 1.5 h / 6.3 - 40 °C / Inert atmosphere

1.2: 10 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 42 °C

2.2: 24 h / 40 - 42 °C

2.3: Amberlite IR-120 (Na)

With pyridine; bis(trichloromethyl) carbonate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; toluene;