carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

Base Information

Chemical Name:carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester
CAS No.:1296133-39-5
Molecular Formula:C₁₆H₂₁ClO₆
Molecular Weight:344.792
Hs Code.:

Synonyms:carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

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Chemical Property of carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

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Technology Process of carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

There total 3 articles about carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1296132-70-1
2-(isopropoxycarbonyloxy)benzaldehyde

: 1296133-39-5
carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

Guidance literature:: 2-(isopropoxycarbonyloxy)benzaldehyde; With pyridine; bis(trichloromethyl) carbonate; In toluene; at 6.3 - 40 ℃; for 1.5h; Inert atmosphere;

In toluene; acetonitrile; at 10 - 20 ℃;

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1296132-70-1
2-(isopropoxycarbonyloxy)benzaldehyde

: 75-65-0
tert-butyl alcohol

: 1296133-39-5
carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

Guidance literature:: bis(trichloromethyl) carbonate; 2-(isopropoxycarbonyloxy)benzaldehyde; With pyridine; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

In tetrahydrofuran; at 44 ℃; for 1h;

tert-butyl alcohol; In tetrahydrofuran; at -10 - 145 ℃; for 48h; Molecular sieve; Inert atmosphere;

Reference yield:

: 90-02-8
salicylaldehyde

: 1296133-39-5
carbonic acid 2-(tert-butoxycarbonyloxy-chloro-methyl)-phenyl ester isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / toluene; acetonitrile / 1 h / 28 °C

2.1: pyridine; bis(trichloromethyl) carbonate / toluene / 1.5 h / 6.3 - 40 °C / Inert atmosphere

2.2: 10 - 20 °C

With pyridine; bis(trichloromethyl) carbonate; potassium carbonate; In toluene; acetonitrile;