sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

Base Information

Chemical Name:sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate
CAS No.:1313591-86-4
Molecular Formula:C₂₂H₂₃O₃S*Na
Molecular Weight:390.479
Hs Code.:

Synonyms:sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

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Chemical Property of sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

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Technology Process of sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

There total 6 articles about sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₈O₅S

: 1313591-86-4
sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

Guidance literature:: C₂₅H₂₈O₅S; With hydrogenchloride; acetic acid; In water; for 12h; Reflux;

With sodium hydroxide; In ethanol; water; for 2h; Reflux;
DOI:10.1016/j.bmc.2011.04.050

Reference yield:

: 1313591-80-8
methyl 2-[3-bromo-4-(chloromethyl)phenyl]propanoate

: 1313591-86-4
sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 12 h / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Reflux

3.1: hydrogenchloride; acetic acid / water / 12 h / Reflux

3.2: 2 h / Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; acetic acid; In tetrahydrofuran; water; acetone; 2.1: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2011.04.050

Reference yield:

: 1313591-81-9
methyl 1-[2-bromo-4-(1-methoxy-1-oxopropan-2-yl)-benzyl]-2-oxocyclopentanecarboxylate

: 1313591-86-4
sodium 2-{4'-(methylthio)-6-[(2-oxocyclopentyl)methyl]biphenyl-3-yl}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Reflux

2.1: hydrogenchloride; acetic acid / water / 12 h / Reflux

2.2: 2 h / Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; acetic acid; In tetrahydrofuran; water; 1.1: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2011.04.050