2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid

Base Information

Chemical Name:2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid
CAS No.:99122-17-5
Molecular Formula:C₈H₈N₄O₂
Molecular Weight:192.177
Hs Code.:2933990090
DSSTox Substance ID:DTXSID80553842
Wikidata:Q82434536
Mol file:99122-17-5.mol

Synonyms:99122-17-5;2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid;2-hydrazinyl-3H-benzimidazole-5-carboxylic acid;1H-Benzimidazole-6-carboxylicacid, 2-hydrazinyl-;1H-Benzimidazole-5-carboxylicacid,2-hydrazino-;2-hydrazinyl-1H-benzo[d]imidazole-5-carboxylic acid;SCHEMBL20819207;DTXSID80553842;AKOS006332383

Suppliers and Price of 2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-HYDRAZINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID 95.00%
5MG
$ 496.38

AccelPharmtech
2-hydrazinyl-1H-Benzimidazole-6-carboxylicacid 97.00%
25G
$ 13300.00

AccelPharmtech
2-hydrazinyl-1H-Benzimidazole-6-carboxylicacid 97.00%
5G
$ 5360.00

AccelPharmtech
2-hydrazinyl-1H-Benzimidazole-6-carboxylicacid 97.00%
1G
$ 3120.00

Total 5 raw suppliers

Chemical Property of 2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid

Chemical Property:

PSA：104.03000
LogP:1.32000
XLogP3:-1.7
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:192.06472551
Heavy Atom Count:14
Complexity:235

Purity/Quality:

99% ^*data from raw suppliers

2-HYDRAZINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C=C1C(=O)O)NC(=N2)NN

Technology Process of 2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid

There total 5 articles about 2-Hydrazinyl-1H-benzimidazole-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 933710-78-2
2- chloro-1H-1,3-benzodiazole-5-carboxylic acid

: 99122-17-5
2-hydrazineyl-1H-benzo[d]imidazole-5-carboxylic acid

Guidance literature:: With hydrazine hydrate; In 1-methyl-pyrrolidin-2-one; at 140 ℃; for 3h; Inert atmosphere;

Reference yield:

: 36692-49-6
Methyl 3,4-diaminobenzoate

: 99122-17-5
2-hydrazineyl-1H-benzo[d]imidazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: trichlorophosphate / 16 h / 100 °C / Inert atmosphere

3: water; sodium hydroxide / ethanol / 16 h / 50 °C

4: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Inert atmosphere

With water; hydrazine hydrate; sodium hydroxide; trichlorophosphate; In 1-methyl-pyrrolidin-2-one; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 106429-57-6
1,3-dihydro-2-oxo-2H-benzimidazole-5-carboxylic acid methyl ester

: 99122-17-5
2-hydrazineyl-1H-benzo[d]imidazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 16 h / 100 °C / Inert atmosphere

2: water; sodium hydroxide / ethanol / 16 h / 50 °C

3: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Inert atmosphere

With water; hydrazine hydrate; sodium hydroxide; trichlorophosphate; In 1-methyl-pyrrolidin-2-one; ethanol;