C₂₃H₁₈ClNO₇

Base Information

Chemical Name:C₂₃H₁₈ClNO₇
CAS No.:1312610-59-5
Molecular Formula:C₂₃H₁₈ClNO₇
Molecular Weight:455.851
Hs Code.:

C<sub>23</sub>H<sub>18</sub>ClNO<sub>7</sub>

Synonyms:C₂₃H₁₈ClNO₇

Suppliers and Price of C₂₃H₁₈ClNO₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₁₈ClNO₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₁₈ClNO₇

There total 5 articles about C₂₃H₁₈ClNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-59-5
C₂₃H₁₈ClNO₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

4.2: Cooling with ice

5.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

With tert.-butylnitrite; sulfuric acid; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-59-5
C₂₃H₁₈ClNO₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

3.2: Cooling with ice

4.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

With tert.-butylnitrite; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: Suzuki Coupling;

Reference yield:

: 4093-31-6
methyl 2-methoxy 4-acetamido 5-chloro benzoate

: 1312610-59-5
C₂₃H₁₈ClNO₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitric acid; sulfuric acid / 1 h / 0 °C

2.1: sulfuric acid / methanol / 7 h / Reflux

3.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

5.2: Cooling with ice

6.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

With tert.-butylnitrite; sulfuric acid; nitric acid; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 4.1: Suzuki Coupling;