ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

Base Information

Chemical Name:ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate
CAS No.:501100-98-7
Molecular Formula:C₃₉H₄₃NO₇
Molecular Weight:637.773
Hs Code.:

Synonyms:ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

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Chemical Property of ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

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Technology Process of ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

There total 2 articles about ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 105-36-2
ethyl bromoacetate

: 188819-44-5
1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl cyanide

: 501100-98-7
ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

Guidance literature:: With zinc; In tetrahydrofuran; Heating;
DOI:10.1055/s-2006-933103

Reference yield: 86.0%

: 105-36-2
ethyl bromoacetate

: (3R,4R,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-carbonitrile

: 501100-98-7
ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

Guidance literature:: With zinc; In tetrahydrofuran; Heating;
DOI:10.1002/1522-2675(200210)85:10<3331::AID-HLCA3331>3.0.CO;2-X

Reference yield: 33.0%

: 620-80-4
ethyl 2-benzylidene acetoacetate

: 501100-98-7
ethyl 3-amino-3-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)propenoate

: 501101-21-9
diethyl (4R)-2-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)-1,4-dihydro-6-methyl-4-phenylpyridine-3,5-dicarboxylate

: 501101-20-8
diethyl (4S)-2-(2',3',4',6'-tetra-O-benzyl-β-D-mannopyranosyl)-1,4-dihydro-6-methyl-4-phenylpyridine-3,5-dicarboxylate

Guidance literature:: With 4 A molecular sieve; In N,N-dimethyl-formamide; at 150 ℃; for 48h;
DOI:10.1002/1522-2675(200210)85:10<3331::AID-HLCA3331>3.0.CO;2-X