Technology Process of C18H17FN2O5
There total 6 articles about C18H17FN2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide; acetonitrile;
at 110 ℃;
for 0.166667h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium nitrate; sulfuric acid / 3.17 h / 0 - 20 °C
2.1: thionyl chloride / 0.5 h / 0 °C / Inert atmosphere
2.2: 18 h / 60 °C / Inert atmosphere
3.1: iron; acetic acid / water; ethanol / 1 h / 110 °C
4.1: N,N-dimethyl-formamide / 0.17 h / Microwave irradiation
5.1: hydrogen; ammonia / methanol / 16 h / 2585.81 Torr
6.1: N,N-dimethyl-formamide; acetonitrile; water / Microwave irradiation; Heating
With
thionyl chloride; sulfuric acid; ammonia; hydrogen; iron; acetic acid; potassium nitrate;
In
methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acsmedchemlett.6b00282
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / 0.5 h / 0 °C / Inert atmosphere
1.2: 18 h / 60 °C / Inert atmosphere
2.1: iron; acetic acid / water; ethanol / 1 h / 110 °C
3.1: N,N-dimethyl-formamide / 0.17 h / Microwave irradiation
4.1: hydrogen; ammonia / methanol / 16 h / 2585.81 Torr
5.1: N,N-dimethyl-formamide; acetonitrile; water / Microwave irradiation; Heating
With
thionyl chloride; ammonia; hydrogen; iron; acetic acid;
In
methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acsmedchemlett.6b00282
