C₂₂H₁₆F₃N₃O₃

Base Information

Chemical Name:C₂₂H₁₆F₃N₃O₃
CAS No.:1276035-82-5
Molecular Formula:C₂₂H₁₆F₃N₃O₃
Molecular Weight:427.383
Hs Code.:

C<sub>22</sub>H<sub>16</sub>F<sub>3</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₂H₁₆F₃N₃O₃

Suppliers and Price of C₂₂H₁₆F₃N₃O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₆F₃N₃O₃

Chemical Property:

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Technology Process of C₂₂H₁₆F₃N₃O₃

There total 5 articles about C₂₂H₁₆F₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20780-53-4
(R)-Styrene oxide

: 1276040-20-0
C₁₃H₁₀F₃N₃O₂

: 149-73-5
trimethyl orthoformate

: 1276035-82-5
C₂₂H₁₆F₃N₃O₃

Guidance literature:: (R)-Styrene oxide; C₁₃H₁₀F₃N₃O₂; With bismuth(III) chloride; In cyclohexane; acetonitrile; at 60 ℃; for 20h; Sealed tube;

trimethyl orthoformate; With trifluoroacetic acid; at 20 ℃; for 1h;

Reference yield:

: 59216-77-2
methyl 5-hydroxy-2-nitro-benzoate

: 1276035-82-5
C₂₂H₁₆F₃N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dimethyl sulfoxide / 100 °C

2.1: ammonia / methanol / 24 h / 100 °C / Sealed tube

3.1: hydrogen / Raney nickel / methanol / 24 h / 20 °C / 775.74 - 1034.32 Torr

4.1: bismuth(III) chloride / cyclohexane; acetonitrile / 20 h / 60 °C / Sealed tube

4.2: 1 h / 20 °C

With bismuth(III) chloride; ammonia; hydrogen; potassium carbonate; Raney nickel; In methanol; cyclohexane; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1007374-52-8
C₁₄H₉F₃N₂O₅

: 1276035-82-5
C₂₂H₁₆F₃N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia / methanol / 24 h / 100 °C / Sealed tube

2.1: hydrogen / Raney nickel / methanol / 24 h / 20 °C / 775.74 - 1034.32 Torr

3.1: bismuth(III) chloride / cyclohexane; acetonitrile / 20 h / 60 °C / Sealed tube

3.2: 1 h / 20 °C

With bismuth(III) chloride; ammonia; hydrogen; Raney nickel; In methanol; cyclohexane; acetonitrile;