[3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester

Base Information

• Chemical Name: [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester
• CAS No.: 262278-14-8
• Molecular Formula: C₂₀H₂₁N₃O₄
• Molecular Weight: 367.404

Synonyms:[3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester

Chemical Property of [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester

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Technology Process of [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester

There total 1 articles about [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-(3-Benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizine-3-carboxylic acid (262278-13-7) → [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester (262278-14-8)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In toluene;

Reference yield:

phosgene (75-44-5) + [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester (262278-14-8) + tert-butyl (2S)-N-benzenesulfonyl-2,3-diaminopropionate (156185-89-6) → (S)-2-Benzenesulfonylamino-3-{3-[7-(3-benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizin-3-yl]-ureido}-propionic acid tert-butyl ester (262278-15-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethyl acetate;

Reference yield:

phosgene (75-44-5) + [3-(7-Amino-6-oxo-6H-quinolizine-3-yloxy)-propyl]-carbamic Acid Benzyl Ester (262278-14-8) + β-amino-3-pyridinepropanoic acid ethyl ester dihydrochloride (149498-96-4,153524-69-7,1217631-87-2) → (+/-)-3-{3-[7-(3-Benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizin-3-yl]-ureido}-3-pyridin-3-yl-propionic acid ethyl ester (262278-16-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

upstream raw materials:

7-(3-Benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizine-3-carboxylic acid

Downstream raw materials:

(S)-2-Benzenesulfonylamino-3-{3-[7-(3-benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizin-3-yl]-ureido}-propionic acid tert-butyl ester

(+/-)-3-{3-[7-(3-Benzyloxycarbonylamino-propoxy)-4-oxo-4H-quinolizin-3-yl]-ureido}-3-pyridin-3-yl-propionic acid ethyl ester

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