2,5-Dioctyloxyanilin

Base Information

• Chemical Name: 2,5-Dioctyloxyanilin
• CAS No.: 77892-63-8
• Molecular Formula: C₂₂H₃₉NO₂
• Molecular Weight: 349.557
• Mol file: 77892-63-8.mol

Synonyms:2,5-Dioctyloxyanilin

Chemical Property of 2,5-Dioctyloxyanilin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Dioctyloxyanilin

There total 2 articles about 2,5-Dioctyloxyanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-Nitro-1,4-bis-octyloxy-benzene (77892-62-7) → 2,5-Dioctyloxyanilin (77892-63-8)

Guidance literature:

With ethanol; iron; ammonium chloride; for 5h; Reflux;

DOI:10.1016/j.tet.2010.11.046

Reference yield:

1,4-bis(octyloxy)benzene (67399-94-4) → 2,5-Dioctyloxyanilin (77892-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 g / HNO₃ (d 1.4) / benzene; acetic acid / 1 h / 45 - 50 °C

2: 82 percent / Fe, glacial AcOH, H₂O / toluene / 6 h / Heating

With water; nitric acid; iron; acetic acid; In acetic acid; toluene; benzene;

Reference yield: 82.0%

2,5-Dioctyloxyanilin (77892-63-8) + trifluoroacetic anhydride (407-25-0) → C24H38F3NO3 (1263321-01-2)

Guidance literature:

With triethylamine; In chloroform; at 0 - 20 ℃;

DOI:10.1016/j.tet.2010.11.046

upstream raw materials:

2-Nitro-1,4-bis-octyloxy-benzene

1,4-bis(octyloxy)benzene

Downstream raw materials:

C₂₂H₃₆O₂NH₂NH₂

C₂₄H₃₇F₃N₂O₅

C₂₄H₃₉F₃N₂O₃

C₅₃H₈₅F₃N₂O₅