2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

Base Information

• Chemical Name: 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl
• CAS No.: 84379-27-1
• Molecular Formula: C₃₀H₂₈Br₂O₃
• Molecular Weight: 596.359

Synonyms:2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

Chemical Property of 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

Chemical Property:

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Technology Process of 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

There total 1 articles about 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,2''-dihydroxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-26-0) + methyl iodide (74-88-4) → 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-27-1)

Guidance literature:

With potassium carbonate;

DOI:10.1039/c39820001219

Reference yield: 68.0%

carbon dioxide (124-38-9,18923-20-1) + 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-27-1) → 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-28-2)

Guidance literature:

metallation;

DOI:10.1039/c39820001219

Reference yield:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-27-1) → 2'-Benzyloxy-3,3''-diisocyanato-2,2''-dimethoxy-5,5',5''-trimethyl-[1,1';3',1'']terphenyl

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / metallation

DOI:10.1039/c39820001219

upstream raw materials:

2,2''-dihydroxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

methyl iodide

Downstream raw materials:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis(bromomethyl)-5,5',5''-trimethyl-1,1':3',1''-terphenyl

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis(hydroxymethyl)-5,5',5''-trimethyl-1,1':3',1''-terphenyl

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarbomethoxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl

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