octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

Base Information

Chemical Name:octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside
CAS No.:130524-08-2
Molecular Formula:C₄₅H₆₆O₉S
Molecular Weight:783.08
Hs Code.:

Synonyms:octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

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Chemical Property of octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

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Technology Process of octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

There total 5 articles about octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 130524-07-1
octyl 2,3-di-O-benzyl-7-deoxy-L-glycero-β-D-gluco-octopyranoside

: 130524-08-2
octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

Guidance literature:: With dmap; In dichloromethane; 1.) from 0 deg C to -18 deg C, 15 h, 2.) RT, 60 min;

Reference yield:

: 111-87-5
octanol

: 130524-08-2
octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / silver zeolite / CH₂Cl₂ / 2 h / Ambient temperature

2: 97 percent / sodium methoxide / methanol / Ambient temperature

3: 74 percent / 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 1.) from 0 deg C to -18 deg C, 15 h, 2.) RT, 60 min

With dmap; silver zeolite; sodium methylate; In methanol; dichloromethane;

Reference yield:

: 130524-05-9
4,6,8-tri-O-acetyl-2,3-di-O-benzyl-7-deoxy-Lglycero-α-D-gluco-octopyranosyl bromide

: 130524-08-2
octyl 2,3-di-O-benzyl-7-deoxy-8-O-(2,4,6-triisopropylbenzenesulfonyl)-L-glycero-β-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / silver zeolite / CH₂Cl₂ / 2 h / Ambient temperature

2: 97 percent / sodium methoxide / methanol / Ambient temperature

3: 74 percent / 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 1.) from 0 deg C to -18 deg C, 15 h, 2.) RT, 60 min

With dmap; silver zeolite; sodium methylate; In methanol; dichloromethane;