1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

Base Information

Chemical Name:1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid
CAS No.:1416133-66-8
Molecular Formula:C₁₂H₁₂N₄O₆S
Molecular Weight:340.316
Hs Code.:

Synonyms:1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

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Chemical Property of 1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

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Technology Process of 1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

There total 3 articles about 1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1192358-10-3
N-(2-azidoethyl)benzenesulfonamide

: 142-45-0
Acetylenedicarboxylic acid

: 1416133-66-8
1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

Guidance literature:: In tetrahydrofuran; for 1h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2012.11.019

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1416133-66-8
1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 4 h / 25 °C

2: sodium azide / 6 h / 80 °C

3: tetrahydrofuran / 1 h / Inert atmosphere; Reflux

With sodium azide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.019

Reference yield:

: 2-(phenylsulfonylamino)ethyl(phenylsulfonate)

: 1416133-66-8
1-[2-(phenylsulfonamido)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / 6 h / 80 °C

2: tetrahydrofuran / 1 h / Inert atmosphere; Reflux

With sodium azide; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.11.019