(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

Base Information

Chemical Name:(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate
CAS No.:1428470-86-3
Molecular Formula:C₂₃H₂₈O₈
Molecular Weight:432.471
Hs Code.:

Synonyms:(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

Chemical Property:

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Technology Process of (R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

There total 3 articles about (R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1428471-06-0
(2S,3R)-tert-butyl 2-benzylamino-3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

: 1428470-86-3
(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

: 100-46-9
benzylamine

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1021/jo400147f

Reference yield:

: C₂₃H₂₉NO₅

: 1428470-86-3
(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

: 100-46-9
benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: zinc trifluoromethanesulfonate / dichloromethane / 9 h / 30 °C

2: samarium diiodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; water / 1 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; zinc trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo400147f

Reference yield:

: 533-31-3
Sesamol

: 1428470-86-3
(R)-tert-butyl 3-(2-hydroxy-4,5-methylenedioxyphenyl)-3-(3,4,5-trimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: zinc trifluoromethanesulfonate / dichloromethane / 9 h / 30 °C

2: samarium diiodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; water / 1 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; zinc trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo400147f