4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

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Chemical Name:4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole
CAS No.:1496532-91-2
Molecular Formula:C₂₈H₂₅BrN₂O₅S₂
Molecular Weight:613.553
Hs Code.:

Synonyms:4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

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Technology Process of 4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

There total 1 articles about 4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 913484-72-7
N-(2-hydroxy-but-3-ynyl)-4-methylbenzenesulfonamide

: 1273005-83-6
2-(4-bromo-1-tosyl-1H-indol-3-yl)acetaldehyde

: 1496532-91-2
4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

Guidance literature:: With iron(III) chloride; In dichloromethane; at 20 - 45 ℃; for 0.2h; Concentration; Temperature; Time; Reagent/catalyst;
DOI:10.1021/jo4023588

Reference yield: 69.0%

: 1496532-91-2
4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

: 1,6-ditosyl-8-formyl-4,5,6,9-tetrahydroindolo[4,3-ef]indole

Guidance literature:: 4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole; With triphenylphosphine; In acetonitrile; for 0.166667h; Inert atmosphere;

With palladium diacetate; In acetonitrile; for 0.25h; Inert atmosphere;

With tetrabutylammomium bromide; water; potassium carbonate; In acetonitrile; at 85 ℃; for 8h; Reagent/catalyst; Concentration; Solvent; Temperature; Time; Inert atmosphere;
DOI:10.1021/jo4023588

Reference yield: 28.0%

: 1496532-91-2
4-bromo-3-(2,5-dihydro-4-formyl-1-tosylpyrrol-2-yl)methyl-1-tosylindole

: 1496532-92-3
1,6-ditosyl-8-formyl-4,5,6,7-tetrahydroindolo[4,3-ef]indole

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; silver carbonate; In toluene; at 80 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jo4023588