1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

Base Information

Chemical Name:1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene
CAS No.:870094-69-2
Molecular Formula:C₂₉H₅₀O₇
Molecular Weight:510.712
Hs Code.:

Synonyms:1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

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Chemical Property of 1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

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Technology Process of 1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

There total 4 articles about 1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 870094-68-1
3-decyloxy-5-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 870094-69-2
1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; for 0.333333h;

3-decyloxy-5-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzaldehyde; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1021/ja054542y

Reference yield:

: 870094-61-4
{3-decyloxy-5-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-phenyl}-methanol

: 870094-69-2
1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

2.1: t-BuOK / tetrahydrofuran / 0.33 h

2.2: 85 percent / tetrahydrofuran / 4 h / 20 °C

With potassium tert-butylate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; 2.2: Wittig reaction;
DOI:10.1021/ja054542y

Reference yield:

: 80755-67-5,58320-73-3
3,6,9,12,15-pentaoxahexadecyl tosylate

: 870094-69-2
1-decyloxy-3-[2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-5-vinyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / potassium carbonate; 18-crown-6 / acetone / Heating

2.1: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

3.1: t-BuOK / tetrahydrofuran / 0.33 h

3.2: 85 percent / tetrahydrofuran / 4 h / 20 °C

With 18-crown-6 ether; potassium tert-butylate; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetone; 3.2: Wittig reaction;
DOI:10.1021/ja054542y