1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione

Base Information Edit

Chemical Name:1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione
CAS No.:1239685-39-2
Molecular Formula:C₁₁H₁₀ClN₃O₂S
Molecular Weight:283.738
Hs Code.:
Mol file:1239685-39-2.mol

Synonyms:1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione Edit

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Technology Process of 1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione

There total 1 articles about 1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 24827-37-0
N-(4-chlorobenzyl)thiourea

: 27738-96-1
chlorocarbonyl isocyanate

: 74-88-4
methyl iodide

: 1239685-39-2
1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione

Guidance literature:: N-(4-chlorobenzyl)thiourea; methyl iodide; In methanol; at 20 ℃; for 5h; Cooling with ice;

chlorocarbonyl isocyanate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h; Cooling with ice;

Reference yield: 88.0%

: 4728-12-5
2,2-dimethyl-5-hydroxymethyl-1,3-dioxane

: 1239685-39-2
1-(4-chlorobenzyl)-6-(methylthio)-1,3,5-triazine-2,4(1H,3H)-dione

: C₁₈H₂₂ClN₃O₄S

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 4h; Cooling with ice; Inert atmosphere;
DOI:10.1016/j.bmcl.2021.128384