4,N,N-triethylbenzenesulfonamide

Base Information

Chemical Name:4,N,N-triethylbenzenesulfonamide
CAS No.:25837-36-9
Molecular Formula:C₁₂H₁₉NO₂S
Molecular Weight:241.354
Hs Code.:

Synonyms:4,N,N-triethylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,N,N-triethylbenzenesulfonamide

Chemical Property:

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Technology Process of 4,N,N-triethylbenzenesulfonamide

There total 7 articles about 4,N,N-triethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 6419-71-2
4-chloro-N,N-diethylbenzenesulfonamide

: 2386-64-3
ethylmagnesium chloride

: 25837-36-9
4,N,N-triethylbenzenesulfonamide

Guidance literature:: With 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate; In tetrahydrofuran; at 0 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.8b02886

Reference yield: 92.0%

: 121-44-8
triethylamine

: sodium p-ethylbenzenesulfinic acid

: 25837-36-9
4,N,N-triethylbenzenesulfonamide

Guidance literature:: With tert.-butylhydroperoxide; iodine; In water; at 80 ℃; for 8h; Sealed tube;
DOI:10.1021/acs.orglett.6b01412

Reference yield: 83.0%

: 649-15-0
N,N-diethyl-4-methylbenzenesulfonamide

: 74-88-4
methyl iodide

: 25837-36-9
4,N,N-triethylbenzenesulfonamide

Guidance literature:: N,N-diethyl-4-methylbenzenesulfonamide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃;

methyl iodide; With d⁽⁴⁾-methanol; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jo001402s