C₉H₁₁NO*ClH

Base Information

Chemical Name:C₉H₁₁NO*ClH
CAS No.:1164111-39-0
Molecular Formula:C₉H₁₁NO*ClH
Molecular Weight:185.653
Hs Code.:

Synonyms:C₉H₁₁NO*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₁NO*ClH

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Technology Process of C₉H₁₁NO*ClH

There total 1 articles about C₉H₁₁NO*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 917-54-4
methyllithium

: 874-90-8
4-methoxybenzonitrile

: 1164111-39-0
C₉H₁₁NO*ClH

Guidance literature:: methyllithium; 4-methoxybenzonitrile; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;

With methanol; In tetrahydrofuran; diethyl ether; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In diethyl ether; tert-butyl methyl ether;
DOI:10.1021/ja903319r

Reference yield: 95.0%

: 1164111-39-0
C₉H₁₁NO*ClH

: 574744-39-1,911373-69-8
(1S)-[1-(4-methoxyphenyl)ethyl]amine hydrochloride

Guidance literature:: With 2,6-bis(3,5-bis(3,7-bis(trifluoromethyl)naphthalen-1-yl)phenyl)-4H-dinaphtho[2,1-d:1',2'-f][1,3,2]dithiazepine 3,3,5,5-tetraoxide; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate; In tert-butyl methyl ether; methyl cyclohexane; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1055/s-0040-1706413

Reference yield: 95.0%

: 1164111-39-0
C₉H₁₁NO*ClH

: 574744-39-1,911373-69-8
(R)-1-(4-methoxyphenyl)ethanamine hydrochloride

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,1'-bis[(S)-4,5-dihydro-3H-binaphtho[2,1-c:1',2'-e]phosphino]ferrocene; hydrogen; In methanol; dichloromethane; at 20 ℃; for 20h; under 7600.51 Torr; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja903319r