2-(1-butenyl)thiobenzanilide

Base Information

• Chemical Name: 2-(1-butenyl)thiobenzanilide
• CAS No.: 119298-24-7
• Molecular Formula: C₁₇H₁₇NS
• Molecular Weight: 267.395
• Mol file: 119298-24-7.mol

Synonyms:2-(1-butenyl)thiobenzanilide

Chemical Property of 2-(1-butenyl)thiobenzanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(1-butenyl)thiobenzanilide

There total 2 articles about 2-(1-butenyl)thiobenzanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2-(1-butenyl)benzanilide (119298-23-6) → 2-(1-butenyl)thiobenzanilide (119298-24-7)

Guidance literature:

With Lawessons reagent; In toluene; for 2h; Heating;

DOI:10.1021/jo00266a016

Reference yield:

2-methyl-N-phenylbenzamide (7055-03-0) → 2-(1-butenyl)thiobenzanilide (119298-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) THF, 0 deg C, 30 min

2: 62 percent / Lawesson's reagent / toluene / 2 h / Heating

With Lawessons reagent; n-butyllithium; In toluene;

DOI:10.1021/jo00266a016

Reference yield:

2-(1-butenyl)thiobenzanilide (119298-24-7) → C25H21NOS (119298-26-9,119364-83-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / benzene / 12 h

2: 64 percent / benzene / 72 h / Heating

With triethylamine; In benzene;

DOI:10.1021/jo00266a016

upstream raw materials:

2-(1-butenyl)benzanilide

2-methyl-N-phenylbenzamide

Downstream raw materials:

C₂₅H₂₁NOS

C₂₅H₂₁NOS

C₂₅H₂₁NOS