Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

Base Information

Chemical Name:Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone
CAS No.:672305-24-7
Molecular Formula:C₂₂H₂₁N₃O₃Si
Molecular Weight:403.513
Hs Code.:

Synonyms:Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

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Technology Process of Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

There total 4 articles about Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 98-88-4
benzoyl chloride

: 672305-17-8
Z-6-trimethylsianyl-hexa-3,5-diyn-2-one 4-nitrophenylhydrazone

: 672305-24-7
Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

Guidance literature:: With aluminium trichloride; In dimethyl sulfoxide; for 2h; Heating;
DOI:10.1016/j.tet.2003.11.036

Reference yield:

: 4526-07-2
1,4-bis(trimethylsilyl)-1,3-butadiyne

: 672305-24-7
Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aluminium trichloride / CH₂Cl₂ / 0.5 h / 0 °C

2: methanol / 4 h / 0 °C

3: 71 percent / aluminium trichloride / dimethylsulfoxide / 2 h / Heating

With aluminium trichloride; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.tet.2003.11.036

Reference yield:

: 37176-72-0
6-trimethylsianyl-hexa-3,5-diyn-2-one

: 672305-24-7
Z-6-trimethylsianyl-hexa-3,5-diyn-2-one N-benzoyl-4-nitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 4 h / 0 °C

2: 71 percent / aluminium trichloride / dimethylsulfoxide / 2 h / Heating

With aluminium trichloride; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.tet.2003.11.036