Technology Process of C15H17BrO2
There total 1 articles about C15H17BrO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
toluene;
for 5h;
Reflux;
Dean-Stark;
DOI:10.1002/anie.201309521
- Guidance literature:
-
ethyl 2-(2-tosylhydrazono)propanoate;
With
tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos;
In
1,4-dioxane;
for 0.166667h;
Inert atmosphere;
C15H17BrO2;
In
1,4-dioxane;
at 110 ℃;
for 5h;
Inert atmosphere;
DOI:10.1002/anie.201309521
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: XPhos; tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide / 1,4-dioxane / 0.17 h / Inert atmosphere
1.2: 5 h / 110 °C / Inert atmosphere
2.1: lithium hydroxide / tetrahydrofuran; water / 5 h / 60 °C
3.1: triethylamine; hydrogen; C38H39IrNOP(1+)*C32H12BF24(1-) / dichloromethane / 10 h / 20 °C / 22801.5 Torr / Inert atmosphere; Glovebox; Autoclave
4.1: hydrogen; C38H39IrNOP(1+)*C32H12BF24(1-) / dichloromethane / 10 h / 20 °C / 22801.5 Torr / Inert atmosphere; Glovebox; Autoclave
With
tris-(dibenzylideneacetone)dipalladium(0); C38H39IrNOP(1+)*C32H12BF24(1-); hydrogen; triethylamine; lithium hydroxide; lithium tert-butoxide; XPhos;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/anie.201309521
