C₂₉H₃₄O₅

Base Information

Chemical Name:C₂₉H₃₄O₅
CAS No.:1352033-68-1
Molecular Formula:C₂₉H₃₄O₅
Molecular Weight:462.586
Hs Code.:

C<sub>29</sub>H<sub>34</sub>O<sub>5</sub>

Synonyms:C₂₉H₃₄O₅

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Chemical Property of C₂₉H₃₄O₅

Chemical Property:

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Technology Process of C₂₉H₃₄O₅

There total 10 articles about C₂₉H₃₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352033-67-0
C₂₇H₃₀O₅

: 1826-67-1
vinyl magnesium bromide

: 1352033-68-1
C₂₉H₃₄O₅

Guidance literature:: C₂₇H₃₀O₅; vinyl magnesium bromide; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; Saturated solution;
DOI:10.1016/j.tetasy.2011.09.012

Reference yield:

: 1352033-61-4
ethyl (E)-5-[4-(benzyloxy)-3-methoxyphenyl]-2-pentenoate

: 1352033-68-1
C₂₉H₃₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 °C / Inert atmosphere

1.2: Saturated solution

2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 3 h / -24 °C / Molecular sieve; Inert atmosphere

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 1 h / 0 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 0 °C / Saturated solution

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 10 h / 20 °C / Cooling with ice; Inert atmosphere

7.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

7.2: Saturated solution

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride; toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 2.1: Sharpless epoxidation;
DOI:10.1016/j.tetasy.2011.09.012

Reference yield:

: 1352033-62-5
(E)-5-[4-(benzyloxy)-3-methoxyphenyl]-2-penten-1-ol

: 1352033-68-1
C₂₉H₃₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 3 h / -24 °C / Molecular sieve; Inert atmosphere

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 1 h / 0 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.2: 0 °C / Saturated solution

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 10 h / 20 °C / Cooling with ice; Inert atmosphere

6.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

6.2: Saturated solution

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride; toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 1.1: Sharpless epoxidation;
DOI:10.1016/j.tetasy.2011.09.012