deuteriodiphenylphosphine

Base Information

• Chemical Name: deuteriodiphenylphosphine
• CAS No.: 18632-84-3
• Molecular Formula: C₁₂H₁₁P
• Molecular Weight: 187.185
• Mol file: 18632-84-3.mol

Synonyms:deuteriodiphenylphosphine

Chemical Property of deuteriodiphenylphosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of deuteriodiphenylphosphine

There total 4 articles about deuteriodiphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diphenylphosphane (829-85-6) → deuteriodiphenylphosphine (18632-84-3)

Guidance literature:

diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h; Green chemistry;

With water-d2; In tetrahydrofuran; hexane; at 20 ℃; for 0.166667h; Green chemistry;

DOI:10.1039/c6gc00903d

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) → deuteriodiphenylphosphine (18632-84-3)

Guidance literature:

With gallium(III) trichloride; Et₃SiD; In chlorobenzene; at 100 ℃; for 16h;

DOI:10.1021/acs.inorgchem.8b01578

Reference yield:

triphenylphosphine (603-35-0) → deuteriodiphenylphosphine (18632-84-3)

Guidance literature:

triphenylphosphine; With lithium; In tetrahydrofuran; Inert atmosphere;

With water-d2; In tetrahydrofuran; Inert atmosphere;

DOI:10.1021/om100216f

upstream raw materials:

diphenylphosphane

deuteromethanol

triphenylphosphine

chloro-diphenylphosphine

Downstream raw materials:

ammonia

diphenylphosphane