9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

Base Information

Chemical Name:9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene
CAS No.:873555-18-1
Molecular Formula:C₆₄H₉₀B₂N₄O₉
Molecular Weight:1081.06
Hs Code.:

Synonyms:9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

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Chemical Property of 9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

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Technology Process of 9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

There total 3 articles about 9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 790257-34-0
9,10-bis[6'-(t-butoxycarbonylamino)hexylaminomethyl]-2-acetylanthracene

: 166821-88-1
5,5-dimethyl-2-(2-bromomethylphenyl)-1,3,2-dioxaborinane

: 873555-18-1
9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide);

Reference yield:

: 790257-33-9
9,10-bis(bromomethyl)-2-acetylanthracene

: 873555-18-1
9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 45 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 25 °C

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 15254-37-2
2-Acetyl-9,10-dimethylanthracene

: 873555-18-1
9,10-bis[[N-6'-(t-butoxycarbonylamino)hexyl-N-[2-(5,5-dimethylborinan-2-yl)benzyl]amino]methyl]-2-acetylanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / chloroform; tetrachloromethane / 2 h / 80 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 45 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 25 °C

With N-Bromosuccinimide; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In tetrachloromethane; chloroform; N,N-dimethyl-formamide;