N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide

Base Information

• Chemical Name: N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide
• CAS No.: 95133-91-8
• Molecular Formula: C₂₂H₂₃NO₆
• Molecular Weight: 397.428

Synonyms:N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide

Chemical Property of N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide

There total 5 articles about N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(3R,4S,5R,6R)-5-hydroxy-6-((4-hydroxy-3-(4-hydroxy-3-isopentylbenzamido)-8-methyl-2-oxo-2H-chromen-7-yl)oxy)-3-methoxy-2,2-dimethyltetrahydro-2H-pyran-4-yl carbamate → N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide (95133-91-8)

Guidance literature:

With acetyl chloride; In ethanol; at 80 ℃; for 2h;

Reference yield:

→ N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide (95133-91-8)

Guidance literature:

With hydrogenchloride; methanol;

DOI:10.1021/ja01589a084 DOI:10.1021/ja01534a037

Reference yield:

3-(4-acetoxy-3-isopentyl-benzoylamino)-4,7-dihydroxy-8-methyl-coumarin → N-(4,7-dihydroxy-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-isopentylbenzamide (95133-91-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01592a100

upstream raw materials:

novobiocin

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