amino>acetaldehyde dimethyl acetal

Base Information

Chemical Name:amino>acetaldehyde dimethyl acetal
CAS No.:95333-87-2
Molecular Formula:C₁₄H₂₃NO₃
Molecular Weight:253.342
Hs Code.:

<N-<3-(4-methoxyphenyl)propyl>amino>acetaldehyde dimethyl acetal

Synonyms:amino>acetaldehyde dimethyl acetal

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Chemical Property of amino>acetaldehyde dimethyl acetal

Chemical Property:

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Technology Process of amino>acetaldehyde dimethyl acetal

There total 4 articles about amino>acetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 95333-86-1
N-(2,2-dimethoxyethyl)-3-(4-methoxyphenyl)propionamide

: 95333-87-2
amino>acetaldehyde dimethyl acetal

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 22 ℃; for 3.5h;
DOI:10.1021/jm00162a008

Reference yield:

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 95333-87-2
amino>acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, pyridine / CH₂Cl₂ / 2.5 h

2: CH₂Cl₂ / 5 - 20 °C

3: 52 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 3.5 h / 22 °C

With pyridine; lithium aluminium tetrahydride; oxalyl dichloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00162a008

Reference yield:

: 15893-42-2
3-(4-methoxyphenyl)propionyl chloride

: 95333-87-2
amino>acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 5 - 20 °C

2: 52 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 3.5 h / 22 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00162a008