(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

Chemical Name:(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride
CAS No.:1181445-39-5
Molecular Formula:C₂₄H₃₃N₂O*Cl
Molecular Weight:400.992
Hs Code.:

Synonyms:(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

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Chemical Property of (S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

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Technology Process of (S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

There total 7 articles about (S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1358742-53-6
(S)-2-(2-(2,6-diisopropylphenylamino)ethylamino)-3-phenylpropan-1-ol

: 149-73-5
trimethyl orthoformate

: 1181445-39-5
(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: (S)-2-(2-(2,6-diisopropylphenylamino)ethylamino)-3-phenylpropan-1-ol; With hydrogenchloride; In methanol; Inert atmosphere;

trimethyl orthoformate; In toluene; at 90 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.11.015

Reference yield: 35.0%

: 1181444-65-4
N-(2-iodoethyl)-2,6-diisopropylbenzenaminium chloride

: 3182-95-4
L-Phenylalaninol

: 122-51-0
orthoformic acid triethyl ester

: 1181445-39-5
(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: With formic acid; at 120 ℃;
DOI:10.1021/ol901189m

Reference yield:

: 1358742-52-5
(S)-N₁-(2,6-diisopropylphenyl)-N₂-(1-hydroxy-3-phenylpropan-2-yl)oxalamide

: 1181445-39-5
(S)-1-(2,6-diisopropylphenyl)-3-(1-hydroxy-3-phenylpropan-2-yl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux

2.1: hydrogenchloride / methanol / Inert atmosphere

2.2: 20 h / 90 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2011.11.015