1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene

Base Information

• Chemical Name: 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene
• CAS No.: 72834-87-8
• Molecular Formula: C₂₀H₂₈O
• Molecular Weight: 284.442

Synonyms:1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene

Chemical Property of 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene

Chemical Property:

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Technology Process of 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene

There total 6 articles about 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

6-methyl-8-(2,6,6-trimethyl-cyclohex-1-enyl)-octa-3,5-dien-7-yn-2-one (72834-86-7) + vinylmagnesium chloride (3536-96-7) → 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene (72834-87-8)

Guidance literature:

In tetrahydrofuran;

Reference yield:

2,2,6-trimethylcyclohexan-1-one (2408-37-9) → 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene (72834-87-8)

Guidance literature:

Multi-step reaction with 5 steps

1: KOH

2: aq. HCO₂H

3: (i) BF₃-Et₂O, (ii) aq. NaOAc, AcOH

4: aq. KOH

With potassium hydroxide; formic acid;

Reference yield:

2,6,6-trimethyl-1-(3'-methyl-but-1'-yn-3'-en-1'-yl)-cyclohex-1-ene (55497-48-8) → 1-[3,7-Dimethyl-nona-1-yne-3,5,8-trien-7-ol-1-yl]-2,6,6-trimethyl-cyclohex-1-ene (72834-87-8)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) BF₃-Et₂O, (ii) aq. NaOAc, AcOH

2: aq. KOH

With potassium hydroxide;

upstream raw materials:

6-methyl-8-(2,6,6-trimethyl-cyclohex-1-enyl)-octa-3,5-dien-7-yn-2-one

vinylmagnesium chloride

2,2,6-trimethylcyclohexan-1-one

2,6,6-trimethyl-1-(3'-methyl-but-1'-yn-3'-en-1'-yl)-cyclohex-1-ene

Downstream raw materials:

1-[3,7-Dimethyl-9-bromo-nona-1-yne-3,5,7-trien-1-yl]-2,6,6-trimethyl-cyclohex-1-ene

1-Brom-3,7-dimethyl-9-(2,6,6-trimethyl-1-cyclohexenyl)-2,4,6-nonatrien-8-in

1-Chlor-3,7-dimethyl-9-(2,6,6-trimethyl-1-cyclohexenyl)-2,4,6-nonatrien-8-in

3,7-Dimethyl-9-(2,6,6-trimethyl-1-cyclohexenyl)-2,4,6-nonatrien-8-in-1-yl-acetat

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