6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene

Base Information

• Chemical Name: 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene
• CAS No.: 78269-39-3
• Molecular Formula: C₃₂H₃₆N₂P₂
• Molecular Weight: 510.599

Synonyms:6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene

Chemical Property of 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene

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Technology Process of 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene

There total 3 articles about 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-dimethyl-1,2-phenylenediamine (3213-79-4) → 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.07,12>docosa-7(12),8,10,1(18),19,21-hexaene (78269-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 78 percent / calcium carbonate / H₂O / 48 h / Heating

2: 1.) HCl, 2.) thionyl chloride / 1) chloroform; 2) reflux, 2 h, chloroform

3: 1.) n-BuLi / 1) -78 deg C, THF, hexane; 2) room temperature, THF

With hydrogenchloride; n-butyllithium; thionyl chloride; calcium carbonate; In water;

DOI:10.1021/ja00403a041

Reference yield:

o-bis-((3-hydroxypropyl)methylamino)benzene (78269-34-8) → 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.07,12>docosa-7(12),8,10,1(18),19,21-hexaene (78269-39-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) HCl, 2.) thionyl chloride / 1) chloroform; 2) reflux, 2 h, chloroform

2: 1.) n-BuLi / 1) -78 deg C, THF, hexane; 2) room temperature, THF

With hydrogenchloride; n-butyllithium; thionyl chloride;

DOI:10.1021/ja00403a041

Reference yield:

1,2-diphenylphosphinobenzene (38023-29-9) + o-bis((3-chloropropyl)methylamino)benzene (78269-35-9) → 6,13-dimethyl-cis-2,17-diphenyl-2,17-diphospha-6,13-diazatricyclo<16.4.0.07,12>docosa-7(12),8,10,1(18),19,21-hexaene (78269-39-3)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1) -78 deg C, THF, hexane; 2) room temperature, THF;

DOI:10.1021/ja00403a041

upstream raw materials:

1,2-diphenylphosphinobenzene

o-bis((3-chloropropyl)methylamino)benzene

o-bis-((3-hydroxypropyl)methylamino)benzene

N,N'-dimethyl-1,2-phenylenediamine

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