2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

Base Information

Chemical Name:2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester
CAS No.:651778-33-5
Molecular Formula:C₄₇H₅₆N₆O₈
Molecular Weight:832.997
Hs Code.:

Synonyms:2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

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Chemical Property of 2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

Chemical Property:

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Technology Process of 2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

There total 3 articles about 2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 98-88-4
benzoyl chloride

: 2,6-bis-(2,6-diamino-hexanoylamino)-hexanoic acid methyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT

: 651778-33-5
2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

Guidance literature:: 2,6-bis-(2,6-diamino-hexanoylamino)-hexanoic acid methyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT; With triethylamine; In dichloromethane; for 1h;

benzoyl chloride; In dichloromethane; for 168h; Further stages.;
DOI:10.1039/b304410f

Reference yield: 13.0%

: 687-64-9,42807-32-9,44977-95-9
DL-lysine methyl ester

: 32513-92-1
Nα,ε-dibenzoyl-D,L-lysine

: 651778-33-5
2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1039/b304410f

Reference yield:

: 2,6-bis-(2,6-bis-tert-butoxycarbonylamino-hexanoylamino)-hexanoic acid methyl ester

: 651778-33-5
2,6-bis-(2,6-bis-benzoylamino-hexanoylamino)-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 45 percent / HCl / CH₂Cl₂; diethyl ether / 48 h

2.1: Et₃N / CH₂Cl₂ / 1 h

2.2: 60 percent / CH₂Cl₂ / 168 h

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1039/b304410f