Technology Process of C30H34NO2(1+)*I(1-)
There total 6 articles about C30H34NO2(1+)*I(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
at 60 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 4 h / 100 °C / Inert atmosphere
2: hydrogen / palladium 10% on activated carbon / 48 h / 20 °C / 760.05 Torr
3: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere
4: potassium carbonate / palladium diacetate; XPhos / acetonitrile; water / 2 h / 90 °C / Inert atmosphere
5: 60 °C / Inert atmosphere
With
hydrogen; potassium carbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; palladium diacetate; XPhos;
In
1,4-dioxane; dichloromethane; water; acetonitrile;
1: Suzuki Coupling / 4: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / toluene; tetrahydrofuran / 1.42 h / -78 °C / Inert atmosphere
1.2: 1 h / -50 - 20 °C
2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 4 h / 100 °C / Inert atmosphere
3.1: hydrogen / palladium 10% on activated carbon / 48 h / 20 °C / 760.05 Torr
4.1: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere
5.1: potassium carbonate / palladium diacetate; XPhos / acetonitrile; water / 2 h / 90 °C / Inert atmosphere
6.1: 60 °C / Inert atmosphere
With
n-butyllithium; hydrogen; potassium carbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; palladium diacetate; XPhos;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;
2.1: Suzuki Coupling / 5.1: Suzuki Coupling;