[6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

Base Information

Chemical Name:[6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal
CAS No.:817631-26-8
Molecular Formula:C₁₆H₂₆O₇
Molecular Weight:330.378
Hs Code.:

Synonyms:[6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

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Chemical Property of [6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

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Technology Process of [6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

There total 2 articles about [6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 7252-83-7
1-bromo-2,2-dimethoxyethane

: 817631-21-3
[2-(methoxyethoxymethoxymethyl)]-6-methoxyphenol

: 817631-26-8
[6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

Guidance literature:: [2-(methoxyethoxymethoxymethyl)]-6-methoxyphenol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

1-bromo-2,2-dimethoxyethane; In N,N-dimethyl-formamide; at 50 ℃; for 5h;
DOI:10.1016/j.tet.2004.09.077

Reference yield:

: 4383-05-5
2-hydroxy-3-methoxybenzyl alcohol

: 817631-26-8
[6-methoxy-2-(methoxyethoxymethoxymethyl)]phenyloxyacetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 47 percent / K₂CO₃ / acetone / 6 h / 0 °C

2.1: NaH / dimethylformamide / 2 h / 20 °C

2.2: 33 percent / dimethylformamide / 5 h / 50 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2004.09.077