tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate

Base Information

• Chemical Name: tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate
• CAS No.: 252872-89-2
• Molecular Formula: C₂₀H₃₂N₂O₄
• Molecular Weight: 364.485

Synonyms:tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate

Chemical Property of tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate

There total 1 articles about tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate (252872-89-2)

Guidance literature:

Reference yield: 89.0%

tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate (252872-89-2) + 6-chlorosulfonyl-1,4-benzodioxane (63758-12-3) → {(1S,2R)-1-Benzyl-3-[cyclopentyloxy-(2,3-dihydro-benzo[1,4]dioxine-6-sulfonyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester (252873-07-7)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2005.05.101

Reference yield: 79.0%

tert-butyl N-(1S,2R)-1-benzyl-3-[(cyclopentyloxy)amino]-2-hydroxypropylcarbamate (252872-89-2) + benzo[1,3]dioxol-5-sulfonyl chloride (115010-10-1) → {(1S,2R)-3-[(Benzo[1,3]dioxole-5-sulfonyl)-cyclopentyloxy-amino]-1-benzyl-2-hydroxy-propyl}-carbamic acid tert-butyl ester (863288-63-5)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2005.05.101

Downstream raw materials:

{(1S,2R)-1-Benzyl-3-[cyclopentyloxy-(2,3-dihydro-benzo[1,4]dioxine-6-sulfonyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester

{(1S,2R)-3-[(Benzo[1,3]dioxole-5-sulfonyl)-cyclopentyloxy-amino]-1-benzyl-2-hydroxy-propyl}-carbamic acid tert-butyl ester

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