α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

Base Information

Chemical Name:α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone
CAS No.:120185-44-6
Molecular Formula:C₁₉H₂₂O₇
Molecular Weight:362.379
Hs Code.:

Synonyms:α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

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Chemical Property of α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

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Technology Process of α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

There total 4 articles about α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24195-22-0
1-(2-hydroxy-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)ethanone

: 3188-13-4
ethyl chloromethyl ether

: 120185-44-6
α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

Guidance literature:: With potassium carbonate; In acetone;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 120185-44-6
α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1: ZnCl₂, HCl gas / diethyl ether / 0 °C / overnight

2: H₂O / 2 h / Heating

3: 85 percent / K₂CO₃ / acetone

4: 85 percent / K₂CO₃ / acetone

With hydrogenchloride; potassium carbonate; zinc(II) chloride; In diethyl ether; water; acetone;

Reference yield:

: 66116-74-3
1-(2,4,5-trihydroxyphenyl)-2-(3,4-dimethoxyphenyl)ethanone

: 120185-44-6
α-hydroxymethyl-3,4-dimethoxybenzyl 2-hydroxy-4,5-dimethoxyphenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / K₂CO₃ / acetone

2: 85 percent / K₂CO₃ / acetone

With potassium carbonate; In acetone;