N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

Base Information

Chemical Name:N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide
CAS No.:1606142-77-1
Molecular Formula:C₂₉H₂₇N₅O₁₀S₂
Molecular Weight:669.693
Hs Code.:

Synonyms:N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

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Chemical Property of N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

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Technology Process of N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

There total 4 articles about N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 42060-32-2
N-benzyl-2-nitrobenzenesulfonamide

: N-benzyl-N-(3-hydroxypropyl)-2,4-dinitrobenzenesulfonamide

: 1606142-77-1
N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 100-39-0
benzyl bromide

: 1606142-77-1
N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; 2: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 1606142-77-1
N-benzyl-N-(3-(N-benzyl-2-nitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfon amide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -78 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046