Technology Process of 4-methoxy-2-morpholin-4-yl-N-(pivaloyloxy)benzamide
There total 3 articles about 4-methoxy-2-morpholin-4-yl-N-(pivaloyloxy)benzamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid;
In
methanol;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ol203353a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
2.1: sodium carbonate / water; ethyl acetate / 20 °C / Inert atmosphere
2.2: 4 h / 0 - 20 °C / Inert atmosphere
3.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 16 h / 20 °C / Inert atmosphere
With
oxalyl dichloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; N,N-dimethyl-formamide; Trimethylacetic acid;
In
methanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/ol203353a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate / water; ethyl acetate / 20 °C / Inert atmosphere
1.2: 4 h / 0 - 20 °C / Inert atmosphere
2.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 16 h / 20 °C / Inert atmosphere
With
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; Trimethylacetic acid;
In
methanol; water; ethyl acetate;
DOI:10.1021/ol203353a
