1,34-Tetratriacontandiol

Base Information

• Chemical Name: 1,34-Tetratriacontandiol
• CAS No.: 34061-58-0
• Molecular Formula: C₃₄H₇₀O₂
• Molecular Weight: 510.929
• Mol file: 34061-58-0.mol

Synonyms:1,34-Tetratriacontandiol

Chemical Property of 1,34-Tetratriacontandiol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,34-Tetratriacontandiol

There total 6 articles about 1,34-Tetratriacontandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

(S)-5-methoxy-3-methyl-5-oxopentanoic acid (63473-60-9) + 18-hydroxystearic acid (3155-42-8) → (S,S)-3,6-Dimethyloctandisaeure-dimethylester (36237-75-9,54423-30-2,54423-31-3,120168-00-5) + 1,34-Tetratriacontandiol (34061-58-0) + (S)-21-Hydroxy-3-methylheneicosansaeure-methylester (83483-71-0)

Guidance literature:

In 1,4-dioxane; methanol; at 40 ℃;

DOI:10.1002/jlac.198219820812

Reference yield:

11-bromoundecanoic acid (2834-05-1) → 1,34-Tetratriacontandiol (34061-58-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 79 percent / methanol / 20 °C

2: 2 N aq. KOH / 12 h / 90 °C

3: 40 percent / methanol; dioxane / 40 °C

With potassium hydroxide; In 1,4-dioxane; methanol;

DOI:10.1002/jlac.198219820812

Reference yield:

azelaic monomethyl ester (2104-19-0) → 1,34-Tetratriacontandiol (34061-58-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 79 percent / methanol / 20 °C

2: 2 N aq. KOH / 12 h / 90 °C

3: 40 percent / methanol; dioxane / 40 °C

With potassium hydroxide; In 1,4-dioxane; methanol;

DOI:10.1002/jlac.198219820812

upstream raw materials:

2-[(11-bromoundecyl)oxy]tetrahydro-2H-pyran

1,12-diiodododecane

1,12-dibromododecane

(S)-5-methoxy-3-methyl-5-oxopentanoic acid

Downstream raw materials:

1,34-Bis-trimethylsilanyloxy-tetratriacontane