diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

Base Information

Chemical Name:diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate
CAS No.:151899-90-0
Molecular Formula:C₃₀H₃₄N₃O₄PS
Molecular Weight:563.657
Hs Code.:

Synonyms:diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

Chemical Property:

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Technology Process of diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

There total 10 articles about diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83682-72-8
γ,γ-dichloropropanol

: 194360-39-9
diethyl 3-bromo-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

: 3-acetylthio-3(1,2,4-triazol-3-yl)propane phosphonic acid

: 151899-90-0
diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

Guidance literature:: With potassium; In tetrahydrofuran;

Reference yield:

: 4851-51-8
diethyl ethynylphosphonate

: 151899-90-0
diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi / tetrahydrofuran

2: H₂ / PtO₂ / propan-2-ol

3: Br₂; n-Bu₃P; Et₃N / CH₂Cl₂

4: 18-crown-6 / tetrahydrofuran

With n-butyllithium; 18-crown-6 ether; tributylphosphine; hydrogen; bromine; triethylamine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; isopropyl alcohol; 1: Addition / 2: Hydrogenation / 3: Bromination / 4: Substitution;
DOI:10.1002/(SICI)1096-9063(199708)50:4<297::AID-PS592>3.0.CO;2-2

Reference yield:

: 24385-94-2
1-trimethylsilyl-1'-diethoxy phosphono ethyne

: 151899-90-0
diethyl 3-acetylthio-3(1-trityl-1,2,4-triazol-3-yl)propane phosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: KF / ethanol

2: n-BuLi / tetrahydrofuran

3: H₂ / PtO₂ / propan-2-ol

4: Br₂; n-Bu₃P; Et₃N / CH₂Cl₂

5: 18-crown-6 / tetrahydrofuran

With potassium fluoride; n-butyllithium; 18-crown-6 ether; tributylphosphine; hydrogen; bromine; triethylamine; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol; 1: Hydrolysis / 2: Addition / 3: Hydrogenation / 4: Bromination / 5: Substitution;
DOI:10.1002/(SICI)1096-9063(199708)50:4<297::AID-PS592>3.0.CO;2-2