(phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate

Base Information

• Chemical Name: (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate
• CAS No.: 123466-32-0
• Molecular Formula: C₇H₇O₃S*C₂₄H₂₁INO
• Molecular Weight: 637.538
• Mol file: 123466-32-0.mol

Synonyms:(phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate

Chemical Property of (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate

There total 3 articles about (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

phenyl(phenylethynyl)iodonium tosylate (79069-32-2) + mesitylenecarbonitrile oxide (2904-57-6) → (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate (123466-32-0)

Guidance literature:

In dichloromethane; for 48h; Ambient temperature;

DOI:10.1039/P19890000827

Reference yield:

[hydroxy(tosyloxy)iodo]benzene (27126-76-7) → (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate (123466-32-0)

Guidance literature:

Multi-step reaction with 2 steps

2: 76 percent / CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;

DOI:10.1039/P19890000827

Reference yield:

phenylacetylene (536-74-3) → (phenyl)[5-phenyl-3-(2,4,6-trimethylphenyl)isoxazol-4-yl]iodonium tosylate (123466-32-0)

Guidance literature:

Multi-step reaction with 2 steps

2: 76 percent / CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;

DOI:10.1039/P19890000827

upstream raw materials:

phenyl(phenylethynyl)iodonium tosylate

mesitylenecarbonitrile oxide

[hydroxy(tosyloxy)iodo]benzene

phenylacetylene

Downstream raw materials:

diethyl-dithiocarbamic acid phenyl ester

4-iodo-5-phenyl-3-(2,4,6-trimethylphenyl)isoxazole

3-mesityl-5-phenylisoxazol-4-yl(phenyl)iodonium iodide

nitrobenzene