3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione

Base Information

• Chemical Name: 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione
• CAS No.: 74691-71-7
• Molecular Formula: C₄₀H₂₈N₈O₂
• Molecular Weight: 652.715

Synonyms:3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione

Chemical Property of 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione

Chemical Property:

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Technology Process of 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione

There total 3 articles about 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,11-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-(5,6-diphenyl-1,2,4-triazin-3-yl)-3-hydroxypyridinium chloride (74691-34-2) → 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.12,6>dodeca-4,8-diene-10,11-dione (74691-71-7)

Guidance literature:

With sodium hydrogencarbonate; In water;

DOI:10.1039/P19800000343

Reference yield:

3-HYDROXYPYRIDINE (109-00-2) → 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.12,6>dodeca-4,8-diene-10,11-dione (74691-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 64.2 percent / 9 h / 130 °C

2: 84 percent / NaHCO₃ / H₂O

With sodium hydrogencarbonate; In water;

DOI:10.1039/P19800000343

Reference yield:

3-chloro-5,6-diphenyl-1,2,4-triazine (34177-11-2) → 3,12-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-3,12-diazatricyclo<5.3.1.12,6>dodeca-4,8-diene-10,11-dione (74691-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 64.2 percent / 9 h / 130 °C

2: 84 percent / NaHCO₃ / H₂O

With sodium hydrogencarbonate; In water;

DOI:10.1039/P19800000343

upstream raw materials:

1-(5,6-diphenyl-1,2,4-triazin-3-yl)-3-hydroxypyridinium chloride

3-HYDROXYPYRIDINE

3-chloro-5,6-diphenyl-1,2,4-triazine

Downstream raw materials:

7-endo-(5,6-diphenyl-1,2,4-triazin-3-yl)-7-azabicyclo<4.3.1>deca-3,8-dien-10-one

(1RS,2RS,6SR,7RS)-11-(5,6-diphenyl-1,2,4-triazin-3-yl)-11-azatricyclo<5.3.1.0^2,6>undeca-3,9-dien-8-one

15-(5,6-diphenyl-1,2,4-triazin-3-yl)-15-azapentacyclo<7.5.1.1^3,6.0^2,7.0^10,14>hexadeca-4,12-dien-8-one

(1RS,9RS,10SR,14RS)-11,15-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)-11,15-diazapentacyclo<7.5.1.1^2,7.0^3,6.0^10,14>heptadeca-4,12-diene-8,17-dione

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